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L. X. 1 Article
Effect of Carrier Gas on the Microstructure and Magnetic Properties of Co Nanoparticles Synthesized by Chemical Vapor Condensation
L. X.
J Korean Powder Metall Inst. 2004;11(1):16-21.
DOI: https://doi.org/10.4150/KPMI.2004.11.1.016
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The nano-sized Co particles were successfully synthesized by chemical vapor condensation (CVC) process using the precursor of cobalt carbonyl (Co_2(CO)_8). The influence of carrier gases on the microstructure and magnetic properties of nanoparticles was investigated by means of XRD, TEM, XPS and VSM. The Co nano-particles with different phases and shapes were synthesized with a change of carrier gas : long string morphologies with coexistence of fcc and hcp structure in Ar carrier gas condition; finer Co core in a mass of cobalt oxide with only fcc structure in He; rod type cobalt oxide phase in Ar+6vol%O_2. The saturation magnetization and coercivity was lower in Co nanoparticles synthesized in He carrier gas, due to their finer size.

Citations

Citations to this article as recorded by  
  • The Fabrication of Cobalt Nanopowder by Sonochemical Polyol Synthesis of Cobalt Hydroxide and Magnetic Separation Method
    Jong Min Byun, Myoung Hwan Choi, Chang Min Shim, Ji Young Kim, Young Do Kim
    Journal of Korean Powder Metallurgy Institute.2015; 22(1): 39.     CrossRef
  • Synthesis of Nano Sized Cobalt Powder from Cobalt Sulfate Heptahydrate by Liquid Phase Reduction
    세환 안, 세훈 김, 진호 이, 현선 홍, 영도 김
    Korean Journal of Materials Research.2011; 21(6): 327~333.     CrossRef

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